By Stanley M. Walas
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Product receiver drums are supplied individually for a slop cut, for toluene, light alkymer, heart alkymer, and a heavy alkymer distillate. Tar is drained from the still at the end of the operation through a water cooler into a bottoms receiver drum which is supplied with a steam coil. From this receiver, the tar is loaded at intervals into 50 gal drums, which are trucked away. In addition to the drums which serve to receive the distillation products during the operation of the column, storage tanks are provided for all except the slop cut which is returned to the still by means of the still feed pump; this pump transfers the mixture from the alkymer wash and surge tank into the still.
1. Process Design A. Books Essential to a Private Library 1. Ludwig, Applied Process Design for Chemical and Petroleum Plants, Gulf, Houston 1977-1983, 3 vols. 2. , McGraw-Hill, New York, 1987. 3. Perry, Green, and Maloney, Perry’s Chemical Engineers Handbook, 1. E. W. Thring, Pilot Plants, Models and Scale-up Methods in Chemical Engineering, McGraw-Hill, New York, 1957. 2. G. Jordan, Chemical Pilot Plant Practice, Wiley-Interscience, New York, 1955. 3. V. Kafarov, Cybernetic Methods in Chemistry and Chemical Engineering, Mir Publishers, Moscow, 1976.
Tank through the orifice mixer. Makeup of caustic is from a dilute caustic storage tank. Spent caustic is intermittently drained off to the sewer. s. tank has an internal weir. The caustic solution settles and is removed at the left of the weir; the alkymer overtlows the weir and is stored in the right-hand portion of the tank until amount sufficient for charging the still has accumulated. DISTILLATlON Separation of the reactor product is effected in a template batch distillation column equipped with a water-cooled condenser and a Dowtherm-heated (650”F, 53 psig) still.